Tangidyne™ Film Thickness Monitor Technology

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Provider of Liquid Based or Vacuum Based High Temperature Crystal Microbalances

The UHT500 system is designed for high temperature coating processes that operate up to 500C. This is a new area of processing that is getting increasingly common throughout the semiconductor, optoelectronic and optics industries.

Standard AT-cut quartz crystals can be used upwards of 150°C with only a moderate instability. As the temperature is increased, however, there is a very steep change of frequency with temperature. That means that a change of as little as 1ºC can cause a frequency shift of 10 or more Hz. The crystal monitor interprets this as coating, leading to a false rate measurement and consequently inaccurate thickness reading.

For temperatures above 150ºC we use a new crystalline material: SuperQuartz. You can find this crystal, and the sensor heads for them, on our SuperQuartz? page,
here. These products are designed for ALD (atomic layer deposition), CVD (chemical vapor deposition), MBE (molecular beam epitaxy), CIGS (copper indium gallium diselenide) solar cell fabrication and even OLED (organic light emitting diode) manufacture.
Quartz Crystal Sensors
UHT500 Shutter Model

UHT500™ Temperature Controlled Vacuum Sensor Heads

If you can't stand the heat, get a UHT500.

 Ever wondered why the manual for your quartz crystal film thickness monitor instructed you to keep the sensor head at 20º C when the monitor itself had no provision of measuring it in the first place? Or did you ever wonder why you should keep the crystal at 20ºC in the first place? Why not 30 or 100 or 500º?

It's surprising that the effect of temperature on the measurement properties of a quartz crystal sensor has not been given the attention it deserves. A device that can measure mass in the picogram levels absolutely needs to be temperature monitored at the very least! But even that is only going halfway. We believe it should be temperature controlled continually, in order to obtain the most accurate film thickness values. And if you want to know more, we suggest you read the papers on temperature measurement in our technical bulletin section
.

To obtain the most accurate film thickness measurements, or the most stable crystal environment for monitoring dielectric coatings, we are offering the ThermaHead™ sensor system (image to the left).

Comprised of a 304 stainless steel quartz crystal sensor head (suitable for 0.550" 5 or 6 MHz quartz crystals, the standard variety), this recently patented design combines a cartridge heater with an air-cooed crystal holder. The action of these two elements allows a set point controller, which receives temperature input from a type K thermocouple embedded in the sensor housing, to add heating as needed to maintain the crystal from a range of 50 to 500º C. 

The air-cooling is an essential ingredient of this system, incidentally. With so much radiant heat present in a typical vacuum coating chamber, there is always the problem of thermal runaway. We use dry compressed air, at room temperature to limit these temperatures. You can also use refrigerated air-cooling to provide even lower operating temperatures (below 50 C)

The typical UHT500™ system is comprised of the following elements:

  1. A temperature controlled sensor head, suitable for one (1) crystal, and complete with heater, air-cooling lines (up to 30" long), embedded type K thermocouple, and shutter (if desired but good only to 300C).
  2. A 2.75" ConFlat™ vacuum flange, with air lines, electrical connections for heater, crystal cable, thermocouple and (if needed) shutter air.
  3. A 19" rack mounted or freestanding set point temperature controller (we currently use Eurotherm™ controllers, but that is subject to change), mated to a variable DC power supply (36VDC max). The controller has an RS232 communications output, but other protocols are also available.
  4. All connecting cables and an instruction manual.

Since many people have unusual requirements for sensor head configurations, most units are custom made. Our base price, however, of $4500 for bare sensors (part number TAN-UHT500) and $5500 for shuttered sensors (part number TAN-UHT500-SH), will get you a turnkey heated system, suitable for use to 10-7 torr operation, and with a 1 year money back warranty.

In the near future, we will have this in a dual sensor head version as well. But, we always welcome customer requests if you need anything special, right now. We will do our best to meet your requirements..

ThermaHead™ systems will work with any standard 5 or 6 MHz quartz crystal controller. All you need to do is hook up the crystal cable from your control unit to the BNC connector on the sensor head feedthrough. Nothing could be simpler.


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